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Sample Preparation

Sampling and sample preparation of refractory metals such as titanium and zirconium is somewhat different from that of steel. Unlike steel samples, hydrogen is not as mobile in this group of materials; therefore, storage in liquid nitrogen or dry ice is not required. However, it is important to keep the sample cool when cutting or sectioning. Sample preparation for oxygen and nitrogen determination has beendifferent from that of hydrogen determination.

***红外池的恒温绝热技术消除了外界环境温度的干扰。安徽美国分析仪采购

美国LECO力可氧氮氢分析仪ONH836（氧氮氢联测仪）系列硬件部分

特点和优势

1、炉头区域LED照明系统

2、炉头快速拆装的粉尘过滤装置

3、装有自动旁路阀的可快速拆装氧水捕集装置

4、**的动态流量补偿（DFC）保证热导池气体流量、压力恒定

5、改进的红外检测池技术

     新红外池的恒温绝热技术消除了外界环境温度的干扰

   长寿命的红外发射光源和无漂移的电路设计保证红外检测池的长期稳定

   氧高低双量程采用3个碳红外检测器，同时检测一氧化碳和二氧化碳，保证准确定量

  6、高效脉冲炉冷却系统

   强力内循环水冷装置

   双直流风扇保证持续冷却，不受电压波动的影响

   新电极炉头设计，提高脉冲炉热交换效率

  7、全自动分析系统（可选）

   自动清扫装置

   20位或100位全自动分析系统

   高速全自动真空除尘装置直接将粉尘排至仪器外部捕集器中，消除环境污染

山西LECO氧氮氢分析仪哪家好Cornerstone氧氮氢分析软件分成4个主要部分：分析、诊断、设定、仪器，界面可快速导航和组织。

氧氮氢分析仪

氧氮氢分析仪是一种用于材料科学领域的仪器，于2016年03月09日启用。

技术指标

测量范围： ON 低氧0.0－300ppm OH 低氧0.0－300ppm 高氧0.0－2% 高氧0.0－2% 低氮0.0―300ppm 低氢0.0－50ppm 高氮0.0－2% 高氢0.0－1000ppm 灵敏度： 氧0.01ppm；氮0.1ppm；氢0.01ppm。

主要功能

该仪器配置有16位微处理器和两个**的分别检测高氧和低氧的 红外检测池。氮和氢通过双重范围的热导检测池测量。分析过程中可自动实现从 低范围到高范围的切换。样品在高功率脉冲炉的石墨坩埚中加热可达3000℃以上 高温，脉冲炉采用循环水冷却。该仪器具有灵敏度高、性能好、测量范围宽和分 析结果准确可靠等优点。ONH-2000氧氮氢分析仪是为快速、准确测定铜、钢、铸 铁、合金、钛、镍、钼、锆、陶瓷和其它无机材料中氧、氮、氢的含量而专门设计 制造的。

Software Features & Benefits

Cornerstone brand software is divided into four main sections—Analysis, Diagnostics, Settings, and Instrument—for simplified navigation and organization. Toolbars, sliders, and drop-down menus makeit easy to set parameters for calibration and data processing. The software also includes real-time ambient monitors, with fully animated system diagrams. Advanced diagnostic features include a thorough digital on-board manual, maintenance animations, photo illustrations, and screen captures that quickly provide the direction needed without having to refer to multiple manuals. also Cornerstone supports extended data archiving and flexible reporting capabilities. 长寿命的红外发射光源和无漂移的电路设计保证红外检测池的长期稳定性。

Sample Preparation

Typically, titanium and zirconium samples are chemically etched to remove surface contamination when oxygen and nitrogen are determined. However, etching can introduce hydrogen into the sample.

ASTM method E 1409 "Determination of Oxygen and Nitrogen in Titanium and Titanium Alloys by the Inert

Gas Fusion Technique", as updated in 1996, permits either etching or abrading (filing) of the test specimen.

ASTM E 1447 "Determination of Hydrogen in Titanium and Titanium Alloys by the Inert Gas Fusion Thermal

Conductivity/Infrared Detection Method" permits surface preparation by abrading (if necessary to remove

contamination). Differences in sample preparation present somewhat of a dilemma regarding simultaneous

determination of O, N, and H in titanium. However, abrading samples with a file to remove surface

contamination will yield accurate O, N, and H results. The ONH836 utilizes a high-power electrode furnace to quickly and efficiently release the target gases from within the sample, which allows for a very rapid simultaneous determination of oxygen, nitrogen, and hydrogen.

新型气路管道减少气路连接阀，使得漏气，断路故障更少。安徽美国分析仪采购

Instrument calibration/drift correction.

a. Login a minimum of 3 Standard replicates.

b. Weigh a ~1.000 gram of a calibration/drift standard, enter the mass and standard identification into appropriate replicate fields.

c. Press the Analyze button on the instrument screen. After a short delay, the loading head slide-block will open.

d. Place the calibration/drift standard into the open port at the top of the loading head.

e. Press the Analyze button on the instrument screen again, the loading head slide-block will close and the lower electrode will open.

安徽美国分析仪采购

上海禹重实业有限公司致力于仪器仪表，是一家服务型的公司。公司业务分为光谱仪，色谱仪，质谱仪，样品前处理等，目前不断进行创新和服务改进，为客户提供良好的产品和服务。公司注重以质量为中心，以服务为理念，秉持诚信为本的理念，打造仪器仪表良好品牌。禹重科技凭借创新的产品、专业的服务、众多的成功案例积累起来的声誉和口碑，让企业发展再上新高。