氧氮氢分析仪的操作过程
氧氮氢分析仪可根据的用户的要求定制。该分析仪配备两个不同灵敏度的探测器,在更多的应用中保证了准确度。
操作简单而且安全。在样品称重以后,样品的重量数据通过电子界面传导至相连的电脑中,也可以在软件界面中手动输入样品的重量。
样品被放置在水平放置的炉子中的低温区域。分析开始以后,炉子开始向上转动,然后样品逐渐落入加热区。通过添加载体气体氮气,氢气被扩散出来并且随载体被传导至一个高灵敏度的热传导测量池。
通常一次测量的时间在3到15分钟之间。在分析的过程中设备可以显示测试信号和设备的参数,从信号的评估到结果在界面上的显示全部自动完成;而测量数据则被传导至LIMS(实验室信息管理系统)中。无需过多的保养和维护,而除尘器和净化管的维护工作也方便。
Oxygen, Nitrogen, and Hydrogen in Refractory Metals
Summary
One of the most critical chemical specifications of titanium alloys is the hydrogen content. Too high of a
hydrogen content can cause hydrides to precipitate, which can lead to embrittlement and subsequent
cracking when the alloy is stressed. Hydrogen pickup typically occurs during downstream processing steps
such as heat treating, pickling, and cleaning.
The LECO ONH836 is a simultaneous oxygen, nitrogen, and hydrogen determinator that utilizes an electrode furnace, inert carrier gas, and both infrared and thermal conductivity detection to meet the analytical needs of the refractory metal industry.
This application note was written specifically for use with the LECO ONH836 series determinator.
Procedure – Powder/Chip Samples
Instrument calibration/drift correction.
Add approximately 0.05 g of *** Graphite Powder to a***Graphite Crucible.
Firmly place the crucible on the lower electrode tip or appropriate autoloader position.
Press the Analyze button on the instrument screen,the lower electrode will close and the analysis sequence will start and end automatically.
Repeat steps 3b through 3i a minimum of three times for each calibration/drift standard used.
Instrument Highlights and Features
Optional Features
Optional boom-mounted touch-screen interface package (M) promotes an ergonomic workspace
Optional Performance Package (P) adds a three-stage carrier gas purification system, and a dual-loop gas dose module
Optional Dual Cooling Package (D) adds an integratedliquid-to-air radiator with dual cooling fans. This DC
option gives the user the choice of liquid-to-liquid cooling, liquid-to-air cooling, or a combination of both
Optional integrated autocleaner (H) automatically cleans the upper electrode and lower electrode tip
Optional 20-sample shuttle loader available
Cornerstone氢氧氮分析软件同时支持***的书记文档格式和可变的报告格式。
Instrument calibration/drift correction
f. Clean the upper and lower electrode manually, or, if applicable, remove the crucible and press the analyze button to clean with the automatic cleaner.
g. Firmly place a graphite crucible on the lower electrode tip.
h. Press the Analyze button on the instrument screen, the lower electrode will close and the analysis sequence will start and end automatically.
i. Repeat steps 3b through 3h a minimum of three times for each calibration/drift standard used.
. Calibrate/drift following the procedure outlined in the operator's instruction manual.
可以旁路的OMI-2 气路强化过滤装置增强了检测器的稳定性,使得分析结果更加准确。北京LECO氧氮氢分析仪哪家好
Procedure – Powder/Chip Samples
Determine the instrument blank.
Press the Analyze button on the instrument screen, the lower electrode will close and the analysis sequence will start and end automatically.
Repeat steps 2b through 2g a minimum of three times.
Set the blank following the procedure outlined in the operator's instruction manual.
Instrument calibration/drift correction.
Login a minimum of three Standard reps.
Weigh approximately *** grams of a calibration/drift standard into a *** Nickel Capsule; enter the mass and standard identification into appropriate rep fields. If applicable, place the nickel capsule in the appropriate autoloader position.
北京LECO氧氮氢分析仪哪家好
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