Procedure - Solid Samples
Press the Analyze button on the instrument screen again, the loading head slide-block will close and the lower electrode will open.
Clean the upper and lower electrode manually, or, if applicable, remove the crucible and press the analyze button to clean with the automatic cleaner
Add approximately 0.05 g of *** Graphite Powder to a *** Graphite Crucible.
Firmly place the crucible on the lower electrode tip or appropriate autoloader position.
Press the Analyze button on the instrument screen, the lower electrode will close and the analysis sequence will start and end automatically
Procedure – Powder/Chip Samples
Determine the instrument blank.
Press the Analyze button on the instrument screen again, the loading head slide-block will close and the lower electrode will open.
Clean the upper and lower electrode either manually or remove the crucible and press the analyze button to clean with an automatic cleaner if applicable.
Add approximately 0.05 g of *** Graphite Powder to a 782-720 Graphite Crucible.
Firmly place the crucible on the lower electrode tip or appropriate autoloader position.
LECO—Your source for total analytical solutions
CS CS 844 and 744 Series: Carbon/Sulfur by Combustion
Carbon and sulfur determination by combustion infrared detection
Quick, accurate, and affordable determination for both production control and research
Calibration, analysis, evaluation, and diagnostic functions accessible via user-friendly brand software
GDS GDS 500A and 850A Atomic Emission Spectrometers
Spectral range from 120 to 800 nm
Continuous profile of concentration/thickness
Large, dynamic range with concentrations from ppm to 100% by weight
Short analysis time (minutes)
Method Selection
Two methods are described in this application note; either method can be used to analyze iron, steel, nickel-, and cobalt-base alloys. The Precision Method is recommended for general use and will provide the best precision and accuracy throughout the typical O, N, and H concentrations found in this group of metals; approximate cycle time is 3.5 minutes. The Fast Track method can be used where speed of analysis is a critical component; for example, when molten metal is being sampled and results are required in the shortest possible time. This method will produce suitable results for most samples; approximate cycle time is 2.25 minutes. As noted above, sampling and sample preparation are key elements to accurate O, N, and Hdetermination as well. It is up to the user to determine which method best meets their needs.
国际**的非色散红外及热导检测器 ,无移动部件,不需要手动调整。
氧氮氢分析仪的常见故障及解决方法:
氧和氮空白值超过20。这是由于气流小,不能将炉子中的空气驱赶出去。可调节气体流量,调节载气压力在0.2~0.4MPa。接通仪器载气,放一个石墨坩埚在下电极上,打开主电源开关,点击软件上的关炉按钮,关闭炉子并等待10s。调节流量调节器,直到流量计a显示为30L/h,打开炉子。调节调节器直到流量计b显示为50L/h,再次关闭炉子。如果以上设置不稳定,则增加流量至100L/h,反复调节直至仪器稳定。 改进的红外检测池技术。浙江元素分析仪价格
无需人工干预的全自动清扫系统。山西LECO氧氮氢分析仪价格
Procedure - Solid Samples
Instrument calibration/drift correction.
Place the calibration/drift standard in a *** Nickel Basket, and if applicable, place the sample into the appropriate autoloader position.
Press the Analyze button on the instrument screen. After a short delay, the loading head slide-block will open.
Note: samples using automation should be placed in the appropriate autoloader position before starting the
analysis sequence. Once the sequence has started, the automatic analysis will start and end automatically.
SamplePreparationSamplingandsamplepreparationofref
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