氧氮氢分析仪的常见故障及解决方法
仪器启动时显示。没有水流。系统分析电流切断,分析停止。这是水流探测器不正常,水泵不工作,管道堵塞。将仪器的右面板取下,观察水流探测器,用手挤压补水塑料水瓶,发现水流正常,显示正常,证明水流探测器正常,管道畅通。启动循环水泵,但分析仪显示没有水流,此时可判定水泵不正常。打开水泵转子密封口,启动泵发现电机正常运转,此时关闭进水,拆下水泵,发现叶轮脱落。经了解,判定是由于外部冷却水停水,仪器内循环水温过高(水温应≤70℃),致使叶轮(叶轮材料PVC)热胀并脱轴。用粘合剂粘合叶轮后再粘于叶轮轴上,待粘合剂凝固后试车,仪器运行正常。 采用三个**的红外器检测氧含量,同时检测CO和CO2,然后在转化为CO2集中检测。江苏元素分析仪价格
Procedure – Powder/Chip Samples
Instrument calibration/drift correction.
Press the Analyze button on the instrument screen. After a short delay, the loading head slide-block will open.
Place the Nickel Capsule containing the sample into the open port at the top of the loading head.
Press the Analyze button on the instrument screen again, the loading head slide-block will close and the lower electrode will open.
Clean the upper and lower electrode either manually or remove the crucible and press the analyze button to clean with an automatic cleaner if applicable.
Method Selection
Two methods are described in this application note; either method can be used to analyze iron, steel, nickel-, and cobalt-base alloys. The Precision Method is recommended for general use and will provide the best precision and accuracy throughout the typical O, N, and H concentrations found in this group of metals; approximate cycle time is 3.5 minutes. The Fast Track method can be used where speed of analysis is a critical component; for example, when molten metal is being sampled and results are required in the shortest possible time. This method will produce suitable results for most samples; approximate cycle time is 2.25 minutes. As noted above, sampling and sample preparation are key elements to accurate O, N, and Hdetermination as well. It is up to the user to determine which method best meets their needs.
Summary
The determination of the amount of oxygen, nitrogen, and hydrogen in iron, steel, nickel-, and cobalt-base alloys represents some of the most important quality metrics for these materials. Oxygen is used to create steel from pig iron by removing excess carbon. Oxygen content must be controlled to limit the amount of carbon monoxide that can be formed during solidification which may cause excessive porosity. Nitrogen is considered both an impurity as well as an important alloying agent. Itcan be present as a nitride or interstitially in its gaseous form. Increased nitrogen content is known to increase yield and tensile strength, thus decreasing ductility and formability. Excessive levels may evolve during solidification thus increasing porosity. High hydrogen content is the primary cause of embrittlement, blistering and flaking due to its high
mobility through the lattice and provides no potential alloying benefits. The ONH836 utilizes a high-power
electrode furnace to quickly and efficiently release the target gases from within the sample, which allows
for a very rapid simultaneous determination of oxygen, nitrogen, and hydrogen.
双直流风扇保证持续冷却,不受电压波动的影响。
氧氮氢分析仪
氧氮氢分析仪是一种用于材料科学领域的仪器,于2016年03月09日启用。
技术指标
测量范围: ON 低氧0.0-300ppm OH 低氧0.0-300ppm 高氧0.0-2% 高氧0.0-2% 低氮0.0―300ppm 低氢0.0-50ppm 高氮0.0-2% 高氢0.0-1000ppm 灵敏度: 氧0.01ppm;氮0.1ppm;氢0.01ppm。
主要功能
该仪器配置有16位微处理器和两个**的分别检测高氧和低氧的 红外检测池。氮和氢通过双重范围的热导检测池测量。分析过程中可自动实现从 低范围到高范围的切换。样品在高功率脉冲炉的石墨坩埚中加热可达3000℃以上 高温,脉冲炉采用循环水冷却。该仪器具有灵敏度高、性能好、测量范围宽和分 析结果准确可靠等优点。ONH-2000氧氮氢分析仪是为快速、准确测定铜、钢、铸 铁、合金、钛、镍、钼、锆、陶瓷和其它无机材料中氧、氮、氢的含量而专门设计 制造的。 上海禹重给您提供各种氧氮氢分析仪,欢迎来电咨询!浙江LECO分析仪厂家报价
Cornerstone氧氮氢分析软件分成4个主要部分:分析、诊断、设定、仪器,界面可快速导航和组织。江苏元素分析仪价格
Instrument Highlights and Features
Optional Features
Optional boom-mounted touch-screen interface package (M) promotes an ergonomic workspace
Optional Performance Package (P) adds a three-stage carrier gas purification system, and a dual-loop gas dose module
Optional Dual Cooling Package (D) adds an integratedliquid-to-air radiator with dual cooling fans. This DC
option gives the user the choice of liquid-to-liquid cooling, liquid-to-air cooling, or a combination of both
Optional integrated autocleaner (H) automatically cleans the upper electrode and lower electrode tip
Optional 20-sample shuttle loader available
江苏元素分析仪价格
SamplePreparationSamplingandsamplepreparationofref
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