氧氮氢分析仪

Procedure – Powder/Chip Samples

Determine the instrument blank.

Press the Analyze button on the instrument screen, the lower electrode will close and the analysis sequence will start and end automatically.

Repeat steps 2b through 2g a minimum of three times.

Set the blank following the procedure outlined in the operator's instruction manual.

Instrument calibration/drift correction.

Login a minimum of three Standard reps.

Weigh approximately *** grams of a calibration/drift standard into a *** Nickel Capsule; enter the mass and standard identification into appropriate rep fields. If applicable, place the nickel capsule in the appropriate autoloader position.

Note: LECO Reference Materia***o not require preparation. See preparation statement on the reference material certificate. Solid Standards may be used to calibrate when chip or powder standards are not available.

长寿命的红外发射光源和无漂移的电路设计保证检测器的长期稳定性。氧氮氢分析仪

力可ONH836氧氮氢分析仪

特征

稳固的炉头试样加载结构

试样加载过程中完全密闭，消除大气的中可能带来的杂质的污染；

简化日常分析所需的炉头进样部分机械维护工作。

可选的自动功能

上下电极自动清扫装置；

20位试样及坩埚自动进样装置。

附加功能及优点

可选六轴可旋转触摸屏幕，增强了操作的工效和直观性；

可选具有压力补偿和温度控制性能的标气检测气路；

新型气路管道减少气路连接阀，使得漏气，断路故障更少；

配置SmartLine Remote远程诊断功能。

进口分析仪优惠价格Cornerstone氧氮氢分析软件分成4个主要部分：分析、诊断、设定、仪器，界面可快速导航和组织。

Oxygen, Nitrogen, and Hydrogen in Refractory Metals

Summary

One of the most critical chemical specifications of titanium alloys is the hydrogen content. Too high of a

hydrogen content can cause hydrides to precipitate, which can lead to embrittlement and subsequent

cracking when the alloy is stressed. Hydrogen pickup typically occurs during downstream processing steps

such as heat treating, pickling, and cleaning.

The LECO ONH836 is a simultaneous oxygen, nitrogen, and hydrogen determinator that utilizes an electrode furnace, inert carrier gas, and both infrared and thermal conductivity detection to meet the analytical needs of the refractory metal industry. 

This application note was written specifically for use with the LECO ONH836 series determinator.

Procedure - Solid Samples

Instrument calibration/drift correction.

Add approximately 0.05 g of *** Graphite Powder to a *** Graphite Crucible.

Firmly place the crucible on the lower electrode tip or appropriate autoloader position.

Press the Analyze button on the instrument screen, the lower electrode will close and the analysis sequence will start and end automatically.

Repeat steps 3b through 3j a minimum of three times for each calibration/drift standard used.

Calibrate/drift following the procedure outlined in the operator's instruction manual.

可以旁路的OMI-2 气路强化过滤装置增强了检测器的稳定性，使得分析结果更加准确。

Procedure – Powder/Chip Samples

Prepare the instrument as outlined in the operator's instruction manual.

Determine the instrument blank.

Login a minimum of three Blank reps.

Press the Analyze button on the instrument screen. After a short delay, the loading head slide-block will open. Insert a *** Nickel Capsule (leave capsule open) into the open port at top of loading head.

Note: samples using automation should be placed in the appropriate autoloader position before starting the analysis sequence. Once the sequence has started, the automatic analysis will start and end automatically.

20位试样自动进样系统。美国LECO分析仪

用户友好界面的Cornerstone™ 软件。氧氮氢分析仪

Procedure – Powder/Chip Samples

Determine the instrument blank.

Press the Analyze button on the instrument screen again, the loading head slide-block will close and the lower electrode will open.

Clean the upper and lower electrode either manually or remove the crucible and press the analyze button to clean with an automatic cleaner if applicable.

Add approximately 0.05 g of *** Graphite Powder to a 782-720 Graphite Crucible.

Firmly place the crucible on the lower electrode tip or appropriate autoloader position.

氧氮氢分析仪