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Sample Preparation

Sampling and sample preparation of refractory metals such as titanium and zirconium is somewhat different from that of steel. Unlike steel samples, hydrogen is not as mobile in this group of materials; therefore, storage in liquid nitrogen or dry ice is not required. However, it is important to keep the sample cool when cutting or sectioning. Sample preparation for oxygen and nitrogen determination has beendifferent from that of hydrogen determination.

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Instrument calibration/drift correction.

a. Login a minimum of 3 Standard replicates.

b. Weigh a ~1.000 gram of a calibration/drift standard, enter the mass and standard identification into appropriate replicate fields.

c. Press the Analyze button on the instrument screen. After a short delay, the loading head slide-block will open.

d. Place the calibration/drift standard into the open port at the top of the loading head.

e. Press the Analyze button on the instrument screen again, the loading head slide-block will close and the lower electrode will open.

安徽美国LECO分析仪采购Cornerstone氧氮氧分析软件允许用户在单一分析界面中完成日常的所有工作，快速而且简单易用。

Procedure – Powder/Chip Samples

Determine the instrument blank.

Press the Analyze button on the instrument screen, the lower electrode will close and the analysis sequence will start and end automatically.

Repeat steps 2b through 2g a minimum of three times.

Set the blank following the procedure outlined in the operator's instruction manual.

Instrument calibration/drift correction.

Login a minimum of three Standard reps.

Weigh approximately *** grams of a calibration/drift standard into a *** Nickel Capsule; enter the mass and standard identification into appropriate rep fields. If applicable, place the nickel capsule in the appropriate autoloader position.

Note: LECO Reference Materia***o not require preparation. See preparation statement on the reference material certificate. Solid Standards may be used to calibrate when chip or powder standards are not available.

氧氮氢分析仪的常见故障及解决方法

供电正常、通讯正常，点击确认键后分析仪不工作。这是没有水流，炉子温度太高或仪器通道电压不正常。如没有水流，炉子温度太高这些信息会显示在显示器画面上，但没有信息显示说明这两项正常。接下来检查仪器通道零位电压，如果比±3V高出1V以上，可能是因为气瓶空了，或者是空气进入到分析仪中。检查并更换化学试剂，如果有空气进入热导池里，热导池的电压就会＜-6V，此时打开右面的门，堵住炉子气体进口，10s后，热导池电压值必然升高。经过逐一排查，**终确认碱石棉有问题，更换后仪器正常。 高级诊断程序包括全数字化的在线操作手册、维护模拟演示、图片说明等提供快速指导。

美国LECO力可氧氮氢分析仪ONH836（氧氮氢联测仪）系列硬件部分

特点和优势

1、炉头区域LED照明系统

2、炉头快速拆装的粉尘过滤装置

3、装有自动旁路阀的可快速拆装氧水捕集装置

4、**的动态流量补偿（DFC）保证热导池气体流量、压力恒定

5、改进的红外检测池技术

     新红外池的恒温绝热技术消除了外界环境温度的干扰

   长寿命的红外发射光源和无漂移的电路设计保证红外检测池的长期稳定

   氧高低双量程采用3个碳红外检测器，同时检测一氧化碳和二氧化碳，保证准确定量

  6、高效脉冲炉冷却系统

   强力内循环水冷装置

   双直流风扇保证持续冷却，不受电压波动的影响

   新电极炉头设计，提高脉冲炉热交换效率

  7、全自动分析系统（可选）

   自动清扫装置

   20位或100位全自动分析系统

   高速全自动真空除尘装置直接将粉尘排至仪器外部捕集器中，消除环境污染

为可**的Cornerstone 氧氮氧分析软件采用触摸屏界面使用户达到分析控制、15法设定、在线诊断、数据报告。山东美国LECO分析仪厂家供应

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Instrument Highlights and Features

Features and Benefits

LED light ring illuminates the furnace area

Choice of either argon or helium carrier gas

Novel electrode design increases heat transfer efficiency for increased stability

Non-touch interface systems are also available

User-friendly brand software

High-Performance Detector Design

Thermostatic construction provides increased protection from ambient temperature fluctuations

Optimized emitter control and detection circuitryimproves the IR cell lifetime and long-term stability,

resulting in superior accuracy and precision

Infrared detection for the determination of oxygen, thermoconductivity detection for the determination

of nitrogen

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