氧氮氢分析仪的优点
采用惰气熔融技术,同时测定氧、氮和氢元素含量
新设计封闭气路系统,优化气路循环,使氧氮氢测量更准确
可采用更廉价的氩气作为载气
催化炉温度可调,使氧的测量更加准确
气路系统都采用电磁阀控制,新增分段式漏气检测
水冷样品加样端口,有效隔绝杂质气体侵入
仪器配置和氧、氮、氢测量范围可灵活选择
新设计的高灵敏度红外检测池和热导池,有极低的检出限
分析时间短
脉冲炉功率高达8.5kw,温度3000℃
颗粒状样品无需胶囊包裹,使用经济实惠
化学试剂及管路隐藏在门后(可移除)
强大的分析软件(支持数据和应用报告导出、增加评论区及其他更多功能)。
单点和多点校正(线性回归)
可采用自来水、冷却循环水机或交换机冷却
新设计的产品可用于各类生产控制和实验室。
Procedure – Powder/Chip Samples
Prepare the instrument as outlined in the operator's instruction manual.
Login a minimum of three Blank reps.
Press the Analyze button on the instrument screen. After a short delay, the loading head slide-block will open. Insert a *** Nickel Capsule (leave capsule open) into the open port at top of loading head.
Note: samples using automation should be placed in the appropriate autoloader position before starting the analysis sequence. Once the sequence has started, the automatic analysis will start and end automatically.
Oxygen, Nitrogen, and Hydrogen in Refractory Metals
Summary
Oxygen and nitrogen are alloying elements in titanium, and are also classified as alpha stabilizing elements as they promote alpha phase alloys. Interstitial oxygen and nitrogen levels can be used to regulate the tensile strength of the material, but due to its high solubility can cause unwanted surface embrittlement. This phenomenon can be leveraged,however, under controlled processing to create surface films that increase surface hardness and wear properties.
Instrument calibration/drift correction.
a. Login a minimum of 3 Standard replicates.
b. Weigh a ~1.000 gram of a calibration/drift standard, enter the mass and standard identification into appropriate replicate fields.
c. Press the Analyze button on the instrument screen. After a short delay, the loading head slide-block will open.
d. Place the calibration/drift standard into the open port at the top of the loading head.
e. Press the Analyze button on the instrument screen again, the loading head slide-block will close and the lower electrode will open.
20位试样自动进样系统。
Sample Preparation
Sampling and sample preparation is an important issue because traditional methods used to obtain samples for oxygen and nitrogen determination are different from those recommended for hydrogen, especially when sampling molten metal. The main difference in steel sampling procedures for oxygen/nitrogen and hydrogen is due to the mobilityof hydrogen. Special precautions must be used when sampling for hydrogen. From molten steel and iron, a sample must be quickly quenched in cold water and chilled in a refrigerant such as liquefied nitrogen or a mixture of acetone and solid carbon dioxide in order to reduce losses of hydrogen from diffusion. Losses of oxygen and nitrogen from diffusion are not a problem. A sample that is taken for hydrogen and
chilled in a refrigerant can also be used for oxygen and nitrogen determination. However, a sample that is typically taken for oxygen and/or nitrogen determination is not suitable for hydrogen determination due to hydrogen loss (diffusion). Surface contamination must be removed by filing or light grinding, using care not to overheat the sample.
***红外池的恒温绝热技术消除了外界环境温度的干扰。上海进口分析仪
Cornerstone氢氧氮分析软件同时支持***的书记文档格式和可变的报告格式。广东LECO氧氮氢分析仪厂家报价
Procedure – Powder/Chip Samples
Determine the instrument blank.
Press the Analyze button on the instrument screen, the lower electrode will close and the analysis sequence will start and end automatically.
Repeat steps 2b through 2g a minimum of three times.
Set the blank following the procedure outlined in the operator's instruction manual.
Instrument calibration/drift correction.
Login a minimum of three Standard reps.
Weigh approximately *** grams of a calibration/drift standard into a *** Nickel Capsule; enter the mass and standard identification into appropriate rep fields. If applicable, place the nickel capsule in the appropriate autoloader position.
广东LECO氧氮氢分析仪厂家报价
SamplePreparationSamplingandsamplepreparationofref
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