湖南美国分析仪厂家直销

氧氮氢分析仪的常见故障及解决方法

供电正常、通讯正常，点击确认键后分析仪不工作。这是没有水流，炉子温度太高或仪器通道电压不正常。如没有水流，炉子温度太高这些信息会显示在显示器画面上，但没有信息显示说明这两项正常。接下来检查仪器通道零位电压，如果比±3V高出1V以上，可能是因为气瓶空了，或者是空气进入到分析仪中。检查并更换化学试剂，如果有空气进入热导池里，热导池的电压就会＜-6V，此时打开右面的门，堵住炉子气体进口，10s后，热导池电压值必然升高。经过逐一排查，**终确认碱石棉有问题，更换后仪器正常。 氧高低双量程采用3个碳红外检测一氧化碳和二氧化碳，保证准确定量。湖南美国分析仪厂家直销

美国LECO力可氧氮氢分析仪ONH836 氧氮氢联测仪系列软件部分

1、用户友好界面的Cornerstone软件

力可**的Cornerstone氧氮氢分析软件采用触摸屏界面使用户可完整的达到分析控制、方法设定、在线诊断、数据报告。Cornerstone氧氮氢分析软件允许用户在单一分析界面中完成日常的所有工作，快速而且简单易用。力可创新的批次和重复样品数据分组功能极大简化了样品结果输出和结果标准偏差的自动计算。减少了繁琐的额外数据处理。

2、软件特点和优势

Cornerstone氧氮氢分析软件分成四个主要部分：分析、诊断、设定、仪器，界面可快速导航和组织。工具条、滑动条和下拉式菜单简化了校正和数据处理的参数设定。分析软件同时包括实时的环境参数的检测，提供完整的系统图表模拟。高级诊断程序包括全数字化的在线操作手册、维护模拟演示、图片说明等提供快速指导。Cornerstone氧氮氢分析软件同时支持***的数据文档格式和可变的报告格式。

湖南美国分析仪厂家直销力可***仪器采用触摸屏技术和在线软件平台，增强了仪器的可操作性、降低了分析成本、节省实验室桌面空间。

Instrument calibration/drift correction.

a. Login a minimum of 3 Standard replicates.

b. Weigh a ~1.000 gram of a calibration/drift standard, enter the mass and standard identification into appropriate replicate fields.

c. Press the Analyze button on the instrument screen. After a short delay, the loading head slide-block will open.

d. Place the calibration/drift standard into the open port at the top of the loading head.

e. Press the Analyze button on the instrument screen again, the loading head slide-block will close and the lower electrode will open.

Instrument Highlights and Features

Features and Benefits

LED light ring illuminates the furnace area

Choice of either argon or helium carrier gas

Novel electrode design increases heat transfer efficiency for increased stability

Non-touch interface systems are also available

User-friendly brand software

High-Performance Detector Design

Thermostatic construction provides increased protection from ambient temperature fluctuations

Optimized emitter control and detection circuitryimproves the IR cell lifetime and long-term stability,

resulting in superior accuracy and precision

Infrared detection for the determination of oxygen, thermoconductivity detection for the determination

of nitrogen

OHN836系列仪器采用惰性熔融法。

氧氮氢分析仪的使用注意事项：

1 、氧氮氢分析仪在初次启用前，应该对连接点、焊点、阀门等进行检漏，以确保空气中的氧不会反渗进入管道及仪器内部，造成测量数值偏高。

2、再次使用仪器前，要进行管道系统净化，将漏入的空气除干净，同时确保连接取样管路时没有漏入空气。

3、样气中氧含量的变化会受管道材质及表面粗糙度影响，因此一般连接管路选用铜管或抛光过的不锈钢管，而不用塑料管、橡胶管等。

4、微量元素分析时，要避免各种管件、阀门、表头等死角对样气造成污染，因此必须尽可能的简化气路系统，连接件死角要小，以防止溶解氧逸出造成污染，使用水封、油封及腊封等设备，才能较好的确保数据的。

**的动态流量补偿（DFC）保证热导池气体流量、压力恒定。湖南美国分析仪厂家直销

***电极炉头设计，提高脉冲炉热交换效率。湖南美国分析仪厂家直销

Sample Preparation

Sampling and sample preparation is an important issue because traditional methods used to obtain samples for oxygen and nitrogen determination are different from those recommended for hydrogen, especially when sampling molten metal. The main difference in steel sampling procedures for oxygen/nitrogen and hydrogen is due to the mobilityof hydrogen. Special precautions must be used when sampling for hydrogen. From molten steel and iron, a sample must be quickly quenched in cold water and chilled in a refrigerant such as liquefied nitrogen or a mixture of acetone and solid carbon dioxide in order to reduce losses of hydrogen from diffusion. Losses of oxygen and nitrogen from diffusion are not a problem. A sample that is taken for hydrogen and

chilled in a refrigerant can also be used for oxygen and nitrogen determination. However, a sample that is typically taken for oxygen and/or nitrogen determination is not suitable for hydrogen determination due to hydrogen loss (diffusion). Surface contamination must be removed by filing or light grinding, using care not to overheat the sample.

湖南美国分析仪厂家直销