氧氮氢分析仪
氧氮氢分析仪是一种用于材料科学领域的仪器,于2016年03月09日启用。
技术指标
测量范围: ON 低氧0.0-300ppm OH 低氧0.0-300ppm 高氧0.0-2% 高氧0.0-2% 低氮0.0―300ppm 低氢0.0-50ppm 高氮0.0-2% 高氢0.0-1000ppm 灵敏度: 氧0.01ppm;氮0.1ppm;氢0.01ppm。
主要功能
该仪器配置有16位微处理器和两个**的分别检测高氧和低氧的 红外检测池。氮和氢通过双重范围的热导检测池测量。分析过程中可自动实现从 低范围到高范围的切换。样品在高功率脉冲炉的石墨坩埚中加热可达3000℃以上 高温,脉冲炉采用循环水冷却。该仪器具有灵敏度高、性能好、测量范围宽和分 析结果准确可靠等优点。ONH-2000氧氮氢分析仪是为快速、准确测定铜、钢、铸 铁、合金、钛、镍、钼、锆、陶瓷和其它无机材料中氧、氮、氢的含量而专门设计 制造的。 高性能的红外检测器配置***恒温绝热技术,消除了外界环境温度的干扰。LECO氧氮氢分析仪厂家直销
Procedure - Solid Samples
Instrument calibration/drift correction.
Add approximately 0.05 g of *** Graphite Powder to a *** Graphite Crucible.
Firmly place the crucible on the lower electrode tip or appropriate autoloader position.
Press the Analyze button on the instrument screen, the lower electrode will close and the analysis sequence will start and end automatically.
Repeat steps 3b through 3j a minimum of three times for each calibration/drift standard used.
Calibrate/drift following the procedure outlined in the operator's instruction manual.
Procedure – Powder/Chip Samples
Instrument calibration/drift correction.
Calibrate/drift following the procedure outlined in the operator's instruction manual.
Login Sample with the appropriate number of reps.
Weigh approximately *** grams of appropriately prepared sample into a *** Nickel Capsule, enter mass and sample identification into appropriate rep fields. If applicable, place the nickel capsule in the
appropriate autoloader position.
Repeat steps 3c through 3i for sample analysis.
Procedure - Solid Samples
Determine the instrument blank.
Repeat steps 2b through 2g a minimum of three times.
Set the blank following the procedure outlined in the operator's instruction manual.
Instrument calibration/drift correction.
Login a minimum of 3 Standard replicates.
Weigh approximately *** grams of a calibration/drift standard, enter the mass and standard identification into appropriate replicate fields.
Note: LECO Reference Materia***o not require preparation.See preparation statement on the reference material certificate.
配置SmartLine® Remote远程诊断功能。
ONH836氧氮氢分析仪
高频燃烧红外检测技分析无机材料中的碳、硫含量。
采用惰性气体保护熔融法,提供各种无机材料、钢铁、有色金属、硬质合金、难熔金属、陶瓷等材料中宽范围的氧氮氢同时分析。
该仪器配置MS Windows®的软件接口,专为触摸屏操作定制。长期的开发研究与客户反馈相结合,这个简单方便的软件使得用户可以快速完整访问仪器控制,分析设置,故障诊断,数据报告, **提高日常分析的效率并节省用户宝贵的时间。 可选的Cornerstone® Mobile软件功能,使得用户可以在手机,便携式电脑及台式电脑上便捷的访问仪器数据,分析曲线图形以及仪器的状态,实现对仪器的遥控。 采用三个**的红外器检测氧含量,同时检测CO和CO2,然后在转化为CO2集中检测。江苏氧氮氢分析仪多少钱
全自动分析系统、打印机、天平、远程诊断。LECO氧氮氢分析仪厂家直销
Sample Preparation
Typically, titanium and zirconium samples are chemically etched to remove surface contamination when oxygen and nitrogen are determined. However, etching can introduce hydrogen into the sample.
ASTM method E 1409 "Determination of Oxygen and Nitrogen in Titanium and Titanium Alloys by the Inert
Gas Fusion Technique", as updated in 1996, permits either etching or abrading (filing) of the test specimen.
ASTM E 1447 "Determination of Hydrogen in Titanium and Titanium Alloys by the Inert Gas Fusion Thermal
Conductivity/Infrared Detection Method" permits surface preparation by abrading (if necessary to remove
contamination). Differences in sample preparation present somewhat of a dilemma regarding simultaneous
determination of O, N, and H in titanium. However, abrading samples with a file to remove surface
contamination will yield accurate O, N, and H results. The ONH836 utilizes a high-power electrode furnace to quickly and efficiently release the target gases from within the sample, which allows for a very rapid simultaneous determination of oxygen, nitrogen, and hydrogen.
LECO氧氮氢分析仪厂家直销SamplePreparationSamplingandsamplepreparationofref
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