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Sample Preparation

Sampling and sample preparation of refractory metals such as titanium and zirconium is somewhat different from that of steel. Unlike steel samples, hydrogen is not as mobile in this group of materials; therefore, storage in liquid nitrogen or dry ice is not required. However, it is important to keep the sample cool when cutting or sectioning. Sample preparation for oxygen and nitrogen determination has beendifferent from that of hydrogen determination.

20位或100位全自动分析系统。新疆LECO分析仪咨询报价

Procedure - Solid Samples

Press the Analyze button on the instrument screen again, the loading head slide-block will close and the lower electrode will open.

Clean the upper and lower electrode manually, or, if applicable, remove the crucible and press the analyze button to clean with the automatic cleaner

Add approximately 0.05 g of *** Graphite Powder to a *** Graphite Crucible.

Firmly place the crucible on the lower electrode tip or appropriate autoloader position.

Press the Analyze button on the instrument screen, the lower electrode will close and the analysis sequence will start and end automatically

氧氮氢分析仪的使用注意事项：

1 、氧氮氢分析仪在初次启用前，应该对连接点、焊点、阀门等进行检漏，以确保空气中的氧不会反渗进入管道及仪器内部，造成测量数值偏高。

2、再次使用仪器前，要进行管道系统净化，将漏入的空气除干净，同时确保连接取样管路时没有漏入空气。

3、样气中氧含量的变化会受管道材质及表面粗糙度影响，因此一般连接管路选用铜管或抛光过的不锈钢管，而不用塑料管、橡胶管等。

4、微量元素分析时，要避免各种管件、阀门、表头等死角对样气造成污染，因此必须尽可能的简化气路系统，连接件死角要小，以防止溶解氧逸出造成污染，使用水封、油封及腊封等设备，才能较好的确保数据的。

Instrument Highlights and Features

Features and Benefits

LED light ring illuminates the furnace area

Choice of either argon or helium carrier gas

Novel electrode design increases heat transfer efficiency for increased stability

Non-touch interface systems are also available

User-friendly brand software

High-Performance Detector Design

Thermostatic construction provides increased protection from ambient temperature fluctuations

Optimized emitter control and detection circuitryimproves the IR cell lifetime and long-term stability,

resulting in superior accuracy and precision

Infrared detection for the determination of oxygen, thermoconductivity detection for the determination

of nitrogen

**的动态流量补偿（DFC）保证热导池气体流量、压力恒定。

氧氮氢分析仪

氧氮氢分析仪是一种用于材料科学领域的仪器，于2016年03月09日启用。

技术指标

测量范围： ON 低氧0.0－300ppm OH 低氧0.0－300ppm 高氧0.0－2% 高氧0.0－2% 低氮0.0―300ppm 低氢0.0－50ppm 高氮0.0－2% 高氢0.0－1000ppm 灵敏度： 氧0.01ppm；氮0.1ppm；氢0.01ppm。

主要功能

该仪器配置有16位微处理器和两个**的分别检测高氧和低氧的 红外检测池。氮和氢通过双重范围的热导检测池测量。分析过程中可自动实现从 低范围到高范围的切换。样品在高功率脉冲炉的石墨坩埚中加热可达3000℃以上 高温，脉冲炉采用循环水冷却。该仪器具有灵敏度高、性能好、测量范围宽和分 析结果准确可靠等优点。ONH-2000氧氮氢分析仪是为快速、准确测定铜、钢、铸 铁、合金、钛、镍、钼、锆、陶瓷和其它无机材料中氧、氮、氢的含量而专门设计 制造的。 可选六轴可旋转触摸屏幕，增强了操作的工效和直观性。湖南美国LECO分析仪供应商

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Procedure – Powder/Chip Samples

Instrument calibration/drift correction.

Add approximately 0.05 g of *** Graphite Powder to a***Graphite Crucible.

Firmly place the crucible on the lower electrode tip or appropriate autoloader position.

Press the Analyze button on the instrument screen,the lower electrode will close and the analysis sequence will start and end automatically.

Repeat steps 3b through 3i a minimum of three times for each calibration/drift standard used.